Table 1 1H NMR Data (300 MHz, CDCL3) for Compounds Ty to TyC 18:1
(Ty) | (TyC2) | (TyC3) | (TyC8) | (TyC10) | (TyC12) | (TyC16) | (TyC18) | (TyC18: 1) | |
|---|---|---|---|---|---|---|---|---|---|
1 | 3.72 (t) | 4.26 (t) | 4.26 (t) | 4.28 (t) | 4.24 (t) | 4.25 (t) | 4.31 (t) | 4.23 (t) | 4.23 (t) |
2 | 2.71 (t) | 2.87 (t) | 2.87 (t) | 2.87 (t) | 2.85 (t) | 2.85 (t) | 2.92 (t) | 2.85 (t) | 2.82 (t) |
4 | 7.11 (d) J4,5 = 8.4 | 7.10 (d) J4,5= 8.4 | 7.07 (d) J4,5= 8.4 | 7.08 (d) J4,5= 8.4 | 7.06 (d) J4,5= 8.4 | 7.04 (d) J4,5= 8.4 | 7.12 (d) J4,5= 8.4 | 7.07 (d) J4,5= 8.4 | 7.09 (d) J4,5= 8.4 |
5 | 6.79 (d) J4,5= 9 | 6.80 (d) J4,5= 9 | 6.80 (d) J4,5= 9 | 6.80 (d) J4,5= 9 | 6.79 J4,5= 9 | 6.80 (d) J4,5= 9 | 6.80 (d) J4,5= 9 | 6.80 (d) J4,5= 9 | 6.80 (d) J4,5= 9 |
6 | 5.50 (s) | 5.50 (s) | 5.50 (s) | 5.50 (s) | 5.50 (s) | 6.00(s) | 5.10 (s) | 5.30 (s) | |
2' | 2.06 (s) | 2.32(q) | 2.33(t) | 2.29 (t) | 2.30(t) | 2.36(t) | 2.30(t) | 2.30(t) | |
3' | 1.13 (t) | 1.60(m) | 1.59 (m) | 1.60 (m) | 1.66(m) | 1.60 (m) | 1.60 (m) | ||
4' | 1.28(m) | 1.25 (m) | 1.26 (m) | 1.32 (m) | 1.25 (m) | 1.25 (m) | |||
(CH2)3 | 1.28(m) | 1.25 (m) | 1.26 (m) | 1.32 (m) | 1.25 (m) | 1.25 (m) | |||
8' | 0.9 (t) | 1.25 (m) | 1.26 (m) | 1.32 (m) | 1.25 (m) | 2.00 (m) | |||
9' | 1.25 (m) | 1.26 (m) | 1.32 (m) | 1.25 (m) | 5.33 (m) | ||||
10' | 0.88 (t) | 1.26 (m) | 1.32 (m) | 1.25 (m) | 5.33 (m) | ||||
11' | 1.26 (m) | 1.32 (m) | 1.25 (m) | 2.00 (m) | |||||
12' | 0.88 (t) | 1.32 (m) | 1.25 (m) | 1.25 (m) | |||||
13' | 1.32 (m) | 1.25 (m) | 1.25 (m) | ||||||
14' | 1.32 (m) | 1.25 (m) | 1.25 (m) | ||||||
(CH2)n | 1.32 (m) | 1.25 (m) | 1.25 (m) | ||||||
Me | 0.94 (t) | 0.87 (t) | 0.87 (t) |