Treat | Hour | 7β-OH*** | 20α-OH*** | 25-OH*** | Triol*** | α-epoxide*** | 7-keto*** | Total amount of COPs |
---|---|---|---|---|---|---|---|---|
C | 1 | n.d.e | 0.18 ± 0.01a | 0.10 ± 0.02bc | n.d.c | 0.17 ± 0.01a | 0.88 ± 0.12bc | 1.33 ± 0.16def |
3 | n.d.e | 0.18 ± 0.01a | 0.09 ± 0.01cd | n.d.c | 0.11 ± 0.02bc | 0.94 ± 0.17b | 1.32 ± 0.21def | |
5 | n.d.e | 0.08 ± 0.03b | 0.08 ± 0.01e | n.d.c | 0.12 ± 0.03b | 1.10 ± 0.11a | 1.38 ± 0.17def | |
10 | n.d.e | 0.03 ± 0.01e | 0.06 ± 0.01e | n.d.c | 0.09 ± 0.03bcd | 0.82 ± 0.08bc | 1.00 ± 0.12efg | |
CL1 | 1 | 5.75 ± 0.40b | 0.05 ± 0.01c | 0.02 ± 0.00fg | n.d.c | 0.08 ± 0.04cdef | 0.09 ± 0.03ef | 5.99 ± 0.48b |
(1:20) | 3 | 0.55 ± 0.02de | 0.002 ± 0.00F | 0.08 ± 0.02de | n.d.c | 0.10 ± 0.06bc | 0.10 ± 0.02ef | 0.83 ± 0.12efgh |
5 | 0.24 ± 0.02de | n.d.f | 0.10 ± 0.01bc | n.d.c | 0.18 ± 0.02a | 0.20 ± 0.09e | 0.72 ± 0.14fgh | |
10 | 0.18 ± 0.04de | n.d.f | 0.11 ± 0.01ab | 0.02 ± 0.01b | 0.12 ± 0.02b | 0.11 ± 0.01ef | 0.54 ± 0.08gh | |
CL2 | 1 | 3.33 ± 0.67c | 0.04 ± 0.00De | 0.02 ± 0.00fg | n.d.c | 0.02 ± 0.01gh | n.d.f | 3.41 ± 0.68c |
(1:100) | 3 | 0.19 ± 0.02de | 0.002 ± 0.00f | 0.01 ± 0.00gh | 0.02 ± 0.01b | 0.03 ± 00.01gh | 0.03 ± 0.01f | 0.28 ± 0.04h |
5 | 0.40 ± 0.08de | 0.002 ± 0.00f | 0.03 ± 0.00fg | 0.03 ± 0.00a | 0.06 ± 0.00defg | 0.04 ± 0.00f | 0.56 ± 0.09gh | |
10 | 0.29 ± 0.02de | n.d.f | 0.03 ± 0.01f | 0.03 ± 0.00a | 0.08 ± 0.01cde | n.d.f | 0.44 ± 0.04gh | |
CO1 | 1 | 6.51 ± 0.97a | 0.05 ± 0.01cd | 0.06 ± 0.01e | n.d.c | 0.04 ± 0.01gh | 0.77 ± 0.08c | 7.43 ± 1.08a |
(1:20) | 3 | 0.65 ± 0.02d | n.d.f | 0.13 ± 0.01a | n.d.c | 0.04 ± 0.01fgh | 0.90 ± 0.13bc | 1.71 ± 0.17d |
5 | 0.49 ± 0.09de | 0.001 ± 0.00f | 0.04 ± 0.01f | n.d.c | 0.02 ± 0.00gh | n.d.f | 0.54 ± 0.11gh | |
10 | 0.21 ± 0.03de | n.d.f | n.d.h | n.d.c | 0.01 ± 0.00h | n.d.f | 0.22 ± 0.03h | |
CO2 | 1 | 3.08 ± 0.33c | 0.04 ± 0.01cde | 0.03 ± 0.01f | n.d.c | 0.02 ± 0.01gh | n.d.f | 3.18 ± 0.35c |
(1:100) | 3 | 0.24 ± 0.02de | n.d.f | 0.06 ± 0.01e | n.d.c | 0.02 ± 0.01gh | 0.33 ± 0.06d | 0.65 ± 0.10gh |
5 | 0.13 ± 0.03de | n.d.f | n.d.h | n.d.c | 0.05 ± 0.01efgh | 0.37 ± 0.02d | 0.55 ± 0.06gh | |
10 | 0.14 ± 0.03de | n.d.f | n.d.h | n.d.c | 0.03 ± 0.01gh | 0.42 ± 0.10d | 0.58 ± 0.13gh |