Table 1 13 C-NMR data and significant 1 H-NMR data of the compound
Position | δC(ppm) | Type | δH(ppm) |
|---|---|---|---|
1 | 30.4 | CH2 | |
2 | 23.9 | CH2 | |
3 | 74.3 | CH | 4.25 (1H, s, OH) |
4 | 37.4 | C | |
5 | 44.4 | CH | |
6 | 17.3 | CH2 | |
7 | 25.8 | CH2 | |
8 | 49.6 | CH | |
9 | 145.9 | C | |
10 | 34.7 | C | |
11 | 118.3 | CH | 5.11 (1H, t) |
12 | 28.6 | CH2 | |
13 | 43.3 | C | |
14 | 51.0 | C | |
15 | 31.3 | CH2 | |
16 | 27.0 | CH2 | |
17 | 47.7 | CH | |
18 | 13.3 | CH3 | |
19 | 21.7 | CH3 | |
20 | 48.4 | CH | |
21 | 177.3 | C | |
22 | 34.7 | CH2 | |
23 | 25.5 | CH2 | |
24 | 125.6 | CH | 5.21 (1H, t) |
25 | 136.4 | C | |
26 | 17.4 | CH3 | 1.61 (3H, s) |
27 | 25.8 | CH3 | 1.65 (3H, s) |
28 | 21.9 | CH3 | 1.21 (3H, s) |
29 | 27.4 | CH3 | 0.90 (3H, s) |
30 | 22.1 | CH3 | 1.16 (3H,s) |
-OCH3 | 59.8 | 3.85 (3H, s) |